What proof to stop distilling?

Answered by Michael Wilson

When it comes to determining the proof at which to stop distilling, there are a few factors to consider. The proof refers to the alcohol by volume (ABV) content of the distillate. Depending on what you’re making and your desired outcome, you can choose to stop collecting the distillate at different ABV levels.

1. Purpose of Distillation:
The purpose of distillation plays a crucial role in determining the proof at which to stop. If you’re distilling spirits like whiskey, rum, or vodka, you may want to collect the distillate until it reaches a specific ABV range to achieve the desired flavor and character. On the other hand, if you’re producing high-proof neutral spirits for further processing or use as a base for other spirits, you may aim for a higher ABV.

2. Legal Requirements:
Different countries and regions have specific regulations regarding the maximum allowable ABV for certain spirits. For example, in the United States, whiskey must be distilled to no more than 160 proof (80% ABV) and entered into the barrel for aging at no more than 125 proof (62.5% ABV). Therefore, it’s essential to be aware of the legal requirements to ensure compliance if you’re producing spirits for commercial purposes.

3. Flavor Considerations:
The flavor profile of the distillate can vary depending on the ABV at which you stop collecting. Generally, higher ABV distillate tends to have a more intense and concentrated flavor, while lower ABV distillate may retain more impurities and exhibit a different character. Experimentation and personal preference play a significant role in determining the sweet spot for your specific product.

4. Experience and Tradition:
Traditionally, distillers have used their experience and sensory evaluation to determine when to stop distilling. They rely on their senses, such as taste, smell, and visual cues, to assess the quality and flavor of the distillate. This hands-on approach allows for adjustments based on individual preferences and the desired end product.

5. Cut Points:
In distillation, the process of separating different components is often divided into three parts: the heads, hearts, and tails. The heads contain volatile compounds and unwanted flavors, while the hearts are the desired distillate with the desired flavors. The tails contain lower boiling point compounds and impurities. By understanding the cut points for heads and tails, you can collect the hearts at the appropriate ABV.

Ultimately, the decision of when to stop distilling depends on your specific goals, legal requirements, flavor preferences, and personal experience. Some distillers choose to stop collecting the distillate when the ABV drops to 10% or below, while others prefer to collect it at higher ABV levels. It’s important to experiment, take notes, and refine your process over time to achieve the desired outcome for your product.